Synthesis and Characterization of 4-chloro-N'-2-(3,3-dimethyl-1,3-dihydro-2H-benzo[f]indol-2-ylidene)-3-oxopropylidene) benzohydrazonamide and 3-(4-chlorophenyl)-1H-1,2,4-triazole
DOI:
https://doi.org/10.24237/ASJ.01.04.681BKeywords:
Heterocyclic, Indole, Schiff bases, Vilsmeier-Haack.Abstract
Six derivatives of 4-Chlorobenzohydrazonamide have been successfully synthesized. The synthesis pathway was divided in two parts, the first part including synthesis of two starting materials 4-Chlorobenzohydrazonamide (3) and 2-(3,3-dimethyl-1,3-dihydro-2H-benzo[f]indol-2-ylidene) malonaldehyde (4). The second part is the synthesis of of indole Schiff base (4) and 3-(4-chlorophenyl)-1H-1,2,4-triazole (6) from (3). The structures of these compounds were characterized by their spectroscopic techniques such as, FT-IR, 1HNMR and 13CNMR.
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